Number of hours
- Lectures 8.0
- Tutorials 8.0
- Laboratory works 12.0
ECTS
ECTS 2.5
Goal(s)
Bibliographic survey and labwork on the principal quantitative electrochemical techniques to study redox phenomena.
LEVEL : advanced lecture in electrochemistry
Contact Jean-Pierre PETIT
Content(s)
Lecture : principles and applications of the voltammetry, step methods and impedance spectroscopy.
PS : apply the fundamental principles on typical examples from the literature.
- Choice of the electrochemical cell (volume, type of working electrode, counter-electrode, geometry of the cell; 2 or 3 electrode cell). Electroactivity domain, ohmic drop, mass transport conditions.
- Voltammetry: impact of the potential sweep rate, the size of the working electrode, the convection (natural and unforced)...
- Impedance spectroscopy : stationarity, linearity ?
- Practical applications of various techniques to study the same electrochemical system.
Prerequisites
Basics in electrochemistry & advanced in electrochemical kinetics
Test
Written exam (2h) + report
Additional Information
Course list
Curriculum->Master-Recherche->Semester 4
Curriculum->EPEE->Semester 4
Curriculum->Master Electrochimie et Procédés->Semester 4
Bibliography
Instrumental methods in electrochemistry. Southampton Electrochemistry Group, Ellis Horwood Limited, 1985.
Electrochimie. Principes, méthodes et applications. A.J. Bard & L.R. Faulkner. traduction : Masson, Paris, 1983.