Phelma Formation 2022

Crystallography - 4PMFMOFM

  • Number of hours

    • Lectures 10.0
    • Projects 0
    • Tutorials 14.0
    • Internship 0
    • Laboratory works 0

    ECTS

    ECTS 2.0

Goal(s)

Course 1 : Crystallography (10h CM- 14hTD)

This course provides an introduction to crystallography. It covers crystal structure and symmetry, with a particular focus on X-ray diffraction. Understanding the structure of a material is often essential to explain its properties. To probe the structure of matter, one can use X-ray, electron, or neutron diffraction.

By the end of the course, students should be able to describe any crystal structure and determine a structure based on the analysis of an X-ray diffraction pattern.

Course: Microstructures and properties (12h CM- 8hTD)
To give information about the links between microstructural parameters (defects, grain size…) and both mechanical properties (hardening, brittleness, plastic deformation) and functional properties (electric, magnetic…) of metals, ceramics and polymers.

Contact Annie ANTONI, Eirini WILHELM, Guillaume PARRY

Content(s)

Course 1 : Crystallography (10h CM- 14hTD)
Summary
1/ Introduction
2/ Direct and recirocal lattices, lattice classification
3/Study of crystal symmetries, space groups, point groups
4/ X-ray scattering
5/ Experimental methods and case studies

Chapters 2 and 3 deal with geometrical crystallography. The importance of the symmetry of crystals will be emphasized. Examples will be analyzed only from a structural point of view. Questions about the origin of a given structure or chemical bonding are out of the scope of the lectures.
Chapters 4 and 5 on X ray scattering are illustrated by tutorials on relevant examples of crystal structure determination.

Course: Microstructures and properties (12h CM- 8hTD)
Crystalline defects: 8h

Dislocations: properties, interactions, movement
Stacking faults, low and high disorientation grain boundaries
Interfaces / interphases

Mechanical property links: 6h

Ductile/brittle behavior
Notion of toughness, crack propagation
Mechanical testing: tension, creep, hardness, fatigue

Functional property links: 6h

Conductivity - point defects
Dielectric constant - bonding polarizability, ferroelectric materials
Optical properties - gaps and defects - forbidden levels
Magnetic properties - defects/coercive field links
Electronic properties



Prerequisites

Course 1 : Crystallography (10h CM- 14hTD)
No presrequisites

Course: Microstructures and properties (12h CM- 8hTD)
Introduction to materials science, Crystallography, Thermodynamic of solutions, phase diagrams

Test

Semester 7 - The exam is given in english only 

Crystallography – Sessions 1 and 2:
Final exam, Weight: 100%, Written exam, Duration: 2 hours.
Only one double-sided A4 sheet of handwritten notes is allowed. A calculator is permitted.



Additional Information

Semester 7 - This course is given in english only EN

Course list
Curriculum->Degree Advanced Materials (AM)->Semester 7
Curriculum->Internationals Cursus->Semester 7

Bibliography

N.W. Ashcroft and N.D. Mermin
Solid State Physics (Holt-Saunders International editions) : chapters 4,5,6,7.

C. Hammond
The Basics of Crystallography and Diffraction (International Union of Crystallography / Oxford Science Publications, 2001).

M. T. Dove
Structure and Dynamics : an atomic view of materials (Oxford series in condensed matter physics, 2003)

B. E. Warren
X-Ray Diffraction ( Dover publications, 1969 first edition, 1990 second edition).

J. Als-Nielsen and D. McMorrow
Elements of Modern X-ray Physics (John Wiley and sons, 2001)